Chemistry Podcast

Saturday, 28 January 2017

Analytical Balance

Analytical Balance

What is an analytical balance?

what is Analytical Balance
Analytical balance is a lab-instrument used to determine mass of any matter very precisely. These analytical balances are very sensitive and expensive lab-instruments, and also upon the accuracy and precision of analytical balance the accuracy of lab-analysis result depends so handle these balances very carefully. Generally used analytical balances are balances with the capacity of 100 gram to 200 gram and the sensitivity of 0.1 milligram to 0.001 milligram. For any quantitative chemical analysis there is need of analytical balance for the weighing of sample for analysis and weighing of reagents for solution preparation. Analytical balance pan used to put sample on it is enclosed in a glass-fitted case, means analytical balance sensitivity requires that it to be protected by the draft shield or enclosure.
analytical balances

Definition of Analytical Balance

Analytical balance is a lab instrument with a scale to measure the mass to a high degree of precision. Generally used analytical balances are balances with the capacity of 100 gram to 200 gram and the sensitivity of 0.1 milligram to 0.001 milligram.

Where are analytical balances used?

Analytical balances are used in labs so also known as ‘Lab Balances’. In labs analytical balances are used for quantitative analysis like for measuring of sample, preparation of standard solutions etc.

How to weigh on an analytical balance?

These are the following steps to start weighing operation on an analytical balance-
  • Wear hand gloves.
  • Open the door of balance and place the container on pan of analytical balance.
  • Now, close the door of the analytical balance and wait for some time.
  • After some time value on balance display or scale get stabilizes, and shows some weight.
  • Now, press the tare button to get 0.0000 gram reading on display.
  • Add the sample until the required weight.
  • Now, close the door and wait for some time.
  • After some time value on balance display or scale get stabilizes, and shows some weight.
  • Record the net weight.
  • Clean the balance after use.

What is analytical balance uncertainty?

Analytical balance uncertainty is the margin of error in weighing, means when making measurements or weighing there is always an element of uncertainty in measurements or weighing. Determination of measurement uncertainty in analytical balance results is an integral part of the balance calibration.

Why should I calibrate my analytical balance?

Calibration of analytical balance is very necessary because balance calibration ensures that weighing balance is precise, correct, truthful, accurate, and satisfies different standards like ISO, GLP, and GMP. Calibration of analytical balances should be documented, as it specifies the quality of measurements. Documented calibration should be performed repeatedly, at some time intervals (like 3months+/-15days). 

How should I calibrate my analytical balance?

You should not calibrate your balance on your own, but it should be calibrated by third party. Means, calibration of balance is performed by third party authorized service technician.  This third party authorized service technician follow a standard procedure, and utilizes some calibration software to calibrate your analytical balance.

What is the analytical balance minimum weight?

Generally minimum weight of analytical balance is not fixed, means it is different for different balances and it depends on different factors like performance of load cell, location of balance, and surrounding environment. Minimum weight is smallest weight that can be measured with accuracy. If we try to measure below this minimum weight, we get results higher relative measurement uncertainty than the required weighing accuracy. So measurements below minimum weight cannot be trusted.
If you want to determine the minimum weight of your balance, you need to assess measurement uncertainty in the working environment.

Analytical balance accuracy and precision – what is the difference and how to test them?

Precision in balances refers to the closeness of two or more measurements to each other, means if we measure 5gram sample and its display shows 5.0001 in 1st time measurement, 5.0000 in 2nd time measurement, 4.9999 in 3rd measurement, and 5.0000 in 4th measurements so all these results (5.0001, 5.0000, 4.9999, and 5.0000) are very close to each other.
Accuracy in balances means how accurate result it gives so, Accuracy in balances refers to the closeness of a measured value to a known value, and Accuracy in balances is based on repeatability, readability, eccentricity and non-linearity. Accuracy of analytical balance can be tested using
  • A traceable calibrated weight also known as external reference weight having a known mass. And these weights are calibrated by third party and come with documented proof.
  • Accuracy of balance must be determined at its location of use.


Do you know ?

What is Analytical Chemistry ?

Analytical chemistry is all about, what an analytical chemist do in an analytical chemistry lab. And simply we can say that analytical chemistry is the branch of chemistry for qualitative analysis and quantitative analysis of compounds and mixtures by using different test methods and techniques like flame tests, chemical tests, precipitation, titration, chromatography, spectroscopy, separation, microscopy etc.
Definition of Analytical Chemistry- Analytical Chemistry is the branch of chemistry deals with the study of material examination to separate out them into different components and identifying all components and how much these components present in material. There are different analytical methods and techniques to perform these tasks... read more

Sunday, 25 December 2016

Catalytic Decomposition of Hydrogen Peroxide H2O2 – Elephant’s Toothpaste Experiment

Catalytic Decomposition of H2O2 – Elephant’s Toothpaste Experiment

Catalytic Decomposition of H2O2 – Elephant’s Toothpaste Experiment
Elephant's toothpaste is a foamy substance formed as a result of rapid decomposition of hydrogen peroxide. Elephant’s toothpaste reaction experiment is generally used for classroom demonstrations as it requires fewer ingredients and makes a "volcano of foam".
Elephant toothpaste

Description:

H2O2 is decomposed by Iodide Ion. Iodide ion is used as a catalyst and these iodide ions come from KI (Potassium Iodide) or NaI (Sodium Iodide). This decomposition reaction liberates water, oxygen and heat.

Materials:

30% H2O2 (Hydrogen Peroxide)
1 Liter Graduated cylinder
KI (Potassium Iodide) or NaI (Sodium Iodide).
Food Color for fun
Liquid Dish Detergent

Procedure:

1.  Pour 50 mL of 30% H2O2 (Hydrogen Peroxide) in 1 L graduated cylinder.
2.  Then, add 3-4 drops of food color in 1 L graduated cylinder to make colored H2O2 solution.
3.  Then, start adding liquid dish detergent or soap from the side of 1 L graduated cylinder to make a small layer of liquid dish detergent or soap over colored H2O2 solution.
4.  With the help of small beaker add KI or NaI in the cylinder containing H2O2 solution. As a result of reaction, oxygen gas generated and this gas creates large amount of colored foam. This foam comes out of graduated cylinder.

Discussion:

Decomposition of H2O2 (Hydrogen Peroxide) yields O2 (oxygen) and H2O (water). Reaction is catalyzed by I- (Iodide Ion); These Iodide Ion comes from KI or NaI

Reaction-

H2O2 (Aq) + I-1 (Aq) ---> H2O (liquid) + IO- (Aq)
IO- (Aq) + H2O2 (Aq) ---> H2O (liquid) +O2 (g) + I- (Aq)

Overall Reaction-

2H2O2 (Aq) ---> 2H2O (liquid) +O2 (g)

Safety:

Wear proper protective equipment likes hand-gloves and safety goggles when preparing and demonstrating this experiment. Remember concentrated H2O2 (Hydrogen Peroxide) can cause burns.

Video of Catalytic Decomposition of H2O2 – Elephant’s Toothpaste Experiment:






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Sunday, 18 December 2016

Chemical Reaction Quiz Part16

  Chemical Reaction Quiz

Science Quiz by www.ChemistryNotesInfo.com
Source www.reddit.com
This Chemical Reaction Quiz part16 is based on chemical reactions.

1. Chemical reaction always gives-

Reactants
A change of state
A different substance
Water
All of the above


2. From given below, 4-balanced chemical equations, which is example of combustion reaction-

2Mg + O2 → 2MgO
2N2 + 3H2 → 2NH3
CaO + H2O → Ca(OH)2
2Na + Cl2 → 2NaCl
2CH4 + 4O2 → 2CO2 + 4H2O


3. To balance a chemical equation, you should need to change-

Chemical Formulas
Direction of the arrow
Coefficients
Subscripts
Superscripts


4. In chemistry, if you try to balance a chemical equation by changing its subscripts, than you change the-

Atomic number
Atomic Mass
Mass of the reactants
Number of molecules of product
Identity of the compound


5. From given below, 4-balanced chemical equations, which is example of double displacement reaction-

NH4Cl → NH3 + HCl
Cd(NO3)2 + Na2S → CdS + 2NaNO3
2Mg + O2 → 2MgO
2H2O2 → 2H2O + O2
2N2 + 3H2 → 2NH3


6. Chemical Reaction, KClO3 → KCl + O2 is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


7. Which scientist first determined that the masses of the reactants and the products in a chemical reaction must be same-

Lavoisier
Galileo
Newton
Archimedes
Pasteur


8. Combination reactions (also known as Synthesis Reaction) always-

Involve an element and an ionic compound
Require oxygen gas
Use only one reactant
Form only one product
form only two product


9. In a chemical reaction, the arrow means-

A reaction is happening
The equation is balanced
The products flow into reactants
The two sides are equal
All of the above


10. In a decomposition reaction-

Energy in the form of light or heat is often released
Reactants are commonly two ionic compounds in the aqueous solution
one of the reactant is generally water
Form only one product
Reactants in the chemical reaction are usually a metal and a nonmetal


Chemical Reactions Quiz

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Sunday, 11 December 2016

Chemical Reactions Quiz Part15

  Chemical Reactions Quiz

Science Quiz by www.ChemistryNotesInfo.com
Chemical Reaction Quiz
This Chemical Reactions Quiz part15 is based on chemical reaction.

1. Chemical Reaction, 2H₂O → 2H₂ + O₂ is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


2. Chemical Reaction, 8Fe + S₈ → 8FeS is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


3. Chemical Reaction, Zn + H₂SO₄ → ZnSO₄ + H₂ is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


4. Chemical Reaction, AgNO₃ + NaCl → AgCl + NaNO₃ is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


5. Chemical Reaction, CH₄ + 2O₂ → CO₂ + 2H₂O is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


6. Chemical Reaction, 2CO + O₂ → 2CO₂ is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


7. Chemical Reaction, Ca(OH)₂ + H₂SO₄ → CaSO₄ + 2H₂O is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


8. Chemical Reaction, Pb + O₂ → PbO₂ is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


9. Chemical Reaction, 2Fe + 6NaBr → 2FeBr₃ + 6Na is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction


10. Chemical Reaction, 2H₂ + O₂ → 2H₂O is a-

Synthesis Reaction
Decomposition Reaction
Combustion Reaction
Single Displacement Reaction
Double Displacement Reaction



Wednesday, 7 December 2016

Science Quiz Part14

Science Quiz on Measuring Devices

Science Quiz by www.ChemistryNotesInfo.com
Science Quiz
This Science Quiz part14 is based on different measuring devices or measuring instruments used in the field of Science.

1. Distance traveled, displacement is measured by:

Taxmeter
Taximeter
Distancemeter
Displacementmeter


2. Surface tension of the liquid is measured by:

Tacheometer
Tintometer
Tensiometer
Tachometer


3. Temperature is measured by:

Thermometer
Thermusmeter
Hygrometer
Hydrometer


4. Ultraviolet light is measured by:

EW Meter
Electromagnetic Wave Meter
UV Meter
VU Meter


5. Very low pressure is measured by:

Pressure Meter
Voltmeter
Viscometer
Vacuum Gauge


6. Viscosity of a fluid is measured by:

Viscosity Meter
Viscometer
Ostwald Viscometer Principle
Viscosity Measurement Devices


7. Electric potential, voltage is measured by:

Voltmeter
Digital DC Voltmeter
Analog Panel Voltmeter
Ammeter


8. Electrical power is measured by:

Ammeter
Wattmeter
Voltmeter
Voltage Meter


9. Wind direction is measured by:
Quiz of Science MCQs

Wind Vane
Weather Vane
Wind Vane Scale
Wind Vane Meter


10. Fermentation is measured by:

fermentometer
Fermometer
Fermentation Meter
Zymometer



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